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- W1806551246 abstract "The 11.7 T 25 Mg, 27 Al, 29 Si, and 11 B MAS NMR spectra are reported for well-characterized grandidierite, (Mg,Fe)Al 3SiBO9, which contains both Al and Mg in fivefold coordination with oxygen. The 25 Mg spectrum is the first to be reported for 5 Mg, and exhibits a quadrupolar lineshape from which the nuclear quadrupolar coupling constant (3.8 6 0.1 MHz), the asymmetry parameter (0.6 6 0.05), and the isotropic chemical shift (55 6 2 ppm) were derived by spectral simulation. These spectroscopic parameters are discussed in terms of the crystallographic geometry of the fivefold-coordinated site." @default.
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- W1806551246 date "1997-06-01" @default.
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- W1806551246 title "MAS NMR study of pentacoordinated magnesium in grandidierite" @default.
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- W1806551246 doi "https://doi.org/10.2138/am-1997-5-606" @default.
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