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• W1807788863 abstract "Single-pulse 13C NMR spectra and spin-lattice relaxation times T1(1H), detected indirectly via 13C carbons, and T1(13C) were measured at 31°C for virgin pelletized and annealed polylactic acid (PLA) samples using the magic-angle spinning technique. The structural relaxation resulting in more regular crystals with narrower conformation distribution and increase in the lamellae thickness and crystallinity brought about by annealing at 100°C was deduced from the narrowing of the 13C NMR lines and proton spin-lattice relaxation times T1(1H). The spin-lattice relaxation times T1(13C) related to the respective carbons of the α-polymorph of PLA are also discussed in the study." @default.
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• W1807788863 date "2015-06-03" @default.
• W1807788863 modified "2023-10-01" @default.
• W1807788863 title "High-Resolution Solid-State NMR Characterization of Morphology in Annealed Polylactic Acid" @default.
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• W1807788863 doi "https://doi.org/10.1080/1023666x.2015.1033831" @default.
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