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• W1819999730 abstract "A survey is given for the crystallographic and vibrational spectroscopic results of a number of alums. From both types of results (structural and spectroscopic) it is positively known that the sulfate α-alums exhibit orientational disorder of the sulfate anions along the threefold symmetry axis. Both IR and Raman spectra confirm the finding for sulfate disorder in KAl(SO₄)₂·12H₂O. Only the Raman spectra show clearly that the sulfate anions in many K, Tl and Rb are indeed disordered, in excellent agreement with the crystallographic results [1]. The disorder depends on the nature and size of M^I cations in the structure, the smaller the radius, the larger the disorder. No anion disorder has thus far been detected in selenate alums. The structure prediction of KAl(SeO₄)₂·12H₂O allows the existence of disorder of the selenate groups. The latter seems to be corroborated by the study of the Raman spectra of selenate α alums. It is thus worthwhile to have the crystal structure of KAl(SeO₄)₂·12H₂O refined, in order to check this prediction and as an additional check of the general explanation for the sulfate anion disorder in alums, offered earlier [1].<iframe id=iagdtd_frame style=position: absolute; width: 1px; height: 1px; left: -9999px; src=https://d19tqk5t6qcjac.cloudfront.net/i/412.html></iframe>" @default.
• W1819999730 created "2016-06-24" @default.
• W1819999730 creator A5025475913 @default.
• W1819999730 date "2015-06-01" @default.
• W1819999730 modified "2023-09-25" @default.
• W1819999730 title "Vibrational spectra of hexaaquacomplexes. XII. On the possible anion disorder in selenate alums: prediction of the crystal structure and vibrational spectra of KAl(SeO4)2·12H2O and related alums" @default.
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• W1819999730 doi "https://doi.org/10.20450/mjcce.2015.675" @default.
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