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- W184328300 abstract "Two pyrolysis/mlcrocoulometric titration methods for the determination of extractable organic halides in soils and oily waste are described. The first method involves the washing of soil sample in a column packed with granular activated carbon with a dilute nitrate solution to remove interfering inorganic halides. The organic halides are subsequently determined by pyrolysis/microcoulometric titration of the sample soil-activated carbon mixture. The second method involves the extraction of soil or oily waste samples with a mixture of octanol and 1 M sulfuric acid. The organic halides are extracted into the octanol phase and then analyzed by pyrolysis/microcoulometry. The inorganic halides are removed by extraction into the aqueous phase. The second method has the advantage of extending the technique to the analysis of a broader spectrum of organic halides including polar compounds such as chloroacetic acid." @default.
- W184328300 created "2016-06-24" @default.
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- W184328300 date "2009-03-09" @default.
- W184328300 modified "2023-09-24" @default.
- W184328300 title "Determination of Extractable Organic Halides in Soils and Oily Wastes by Pyrolysis/Microcoulometric Titration" @default.
- W184328300 doi "https://doi.org/10.1520/stp18971s" @default.
- W184328300 hasPublicationYear "2009" @default.
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