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- W1855299984 abstract "A novel protocol for the transamidation of DMF and derivatives with weakly nucleophilic anilines has been developed, utilizing a catalytic amount of Pd(OAc)2 and 2,2′-bipyridine, and with PivOH and BF3·Et2O as additives. This methodology has a broad substrate scope, and various corresponding transamidation products were prepared in good to excellent yields from commercially available DMF derivatives and anilines. The synthetic utility of the reported protocol was further demonstrated with a gram-scale experiment. Control experiments suggested the efficient transformation of DMF and derivatives with anilines might owe to the synergistic effect of palladium complex, PivOH, and BF3·Et2O." @default.
- W1855299984 created "2016-06-24" @default.
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- W1855299984 date "2015-12-01" @default.
- W1855299984 modified "2023-10-17" @default.
- W1855299984 title "Synthesis of N-arylcarboxamides by the efficient transamidation of DMF and derivatives with anilines" @default.
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- W1855299984 doi "https://doi.org/10.1016/j.tet.2015.10.008" @default.
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