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- W1856735880 abstract "Poly(styrene-co-maleic anhydride) was imidized with ammonium hydroxide and palm oil, resulting in an aqueous dispersion of hybrid nanoparticles with diameters 85-180 nm (dispersed) or 20-50 nm (dried). The reaction conditions were optimized for different precursors by evaluating the relative amount ammonium hydroxide and maximizing the incorporated palm oil up to 70 wt.%. The interactions between palm oil and polymer phase have been studied by TEM, IR, Raman spectroscopy and thermal analysis (TGA, [TM] DSC). From Raman spectra, the amount of imide and reacted oil were quantified. Through concurring effects of imidization and coupling of fatty acids, the imidization needs a slight excess of NH3 relatively to maleic anhydride. The oxidative stability highly depends on oxidative crosslinking of free or non-reacted oil. Comparing the imide content from spectroscopic and thermal analysis suggests that a complex rigid imide phase without strong relaxation behavior has formed in combination with oil." @default.
- W1856735880 created "2016-06-24" @default.
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- W1856735880 date "2015-05-19" @default.
- W1856735880 modified "2023-09-30" @default.
- W1856735880 title "Hybrid palm-oil/styrene-maleimide nanoparticles synthesized in aqueous dispersion under different conditions" @default.
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- W1856735880 doi "https://doi.org/10.3109/02652048.2015.1028493" @default.
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