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- W1880231673 abstract "The title compound, propane-1,3-diammonium tetravanadate, (C3H12N2)[V4O10], represents a second polymorph of composition beta-[H3N(CH2)3NH3][V4O(10)]. It differs from the alpha polymorph [Riou & Ferey (1995). J. Solid State Chem. 120, 137-145] in the conformation of the propane-1,3-diammonium dication which, in the present example, lies on a twofold axis and adopts a syn-syn rather than a syn-anti conformation. The twofold symmetry of this conformation thus co-operates with the vanadium oxide framework to result in a higher symmetry for the resultant crystal, viz. C2/c versus P2(1)/n. The overall unit-cell parameters for the two polymorphs are similar, and the inorganic layer within each is topologically identical, comprising edge-sharing V(IV)O5 square pyramids linked together via corner-sharing with V(V)O4 tetrahedra. A key difference between the two polymorphs is a ;head-to-head' versus ;head-to-tail' stacking of the vanadyl groups in adjacent layers." @default.
- W1880231673 created "2016-06-24" @default.
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- W1880231673 date "2006-10-31" @default.
- W1880231673 modified "2023-09-27" @default.
- W1880231673 title "A second polymorph of [H<sub>3</sub>N(CH<sub>2</sub>)<sub>3</sub>NH<sub>3</sub>][V<sub>4</sub>O<sub>10</sub>]" @default.
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- W1880231673 doi "https://doi.org/10.1107/s0108270106040777" @default.
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