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- W1892632514 abstract "Abstract The one‐pot regioselective consecutive multihalogenation of 2,2′‐bithiophene ( 1 ) was demonstrated. Compound 1 was consecutively halogenated with lithium halides such as lithium bromide, chloride, and/or iodide in the presence of lead tetraacetate in chloroform at room temperature or under reflux conditions to give 5‐bromo(or chloro)‐5′‐iodo(or chloro)‐, 3‐bromo(or chloro)‐5,5′‐dibromo(or dichloro, diiodo)‐, 3,3′‐dibromo‐(or dichloro)‐5,5′‐diiodo(or dibromo, dichloro)‐, and 3,3′,5‐tribromo(or trichloro)‐5′‐iodo(or bromo)‐2,2′‐bithiophenes. Notably, this process offers a regioselective method for consecutive multihalogenation in one pot, and the yields and selectivity are also higher than those obtained in the step‐by‐step and concurrent halogenation methods." @default.
- W1892632514 created "2016-06-24" @default.
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- W1892632514 date "2013-04-09" @default.
- W1892632514 modified "2023-10-12" @default.
- W1892632514 title "One-Pot, Regioselective Consecutive Multihalogenation of 2,2′-Bithiophene" @default.
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- W1892632514 doi "https://doi.org/10.1002/ejoc.201300379" @default.
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