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- W1903441 abstract "An extraction clean-up method is described which is suitable for a wide range of pesticides on non-fatty crops. It is based on methanol extraction followed by toluene/saline partitioning and activated C/cellulose/Florisil clean-up. Residues are determined by GC with electron capture or alkali flame ionisation detection. Confirmation uses Capillary GC/MS of fractions further purified on silica gel. A magnetic sector instrument has been coupled to a capillary column GC by an open split interface. Data acquisition and processing is by a minicomputer based data system. Examples of its use are provided by the identification of metabolites of the fungicide vinclozolin on kiwi fruit and the soil insecticide isazophos in ryegrass. The presence of 2,4,5-T butyl esters in a batch of contaminated butter was also confirmed using the system." @default.
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- W1903441 date "1983-01-01" @default.
- W1903441 modified "2023-09-23" @default.
- W1903441 title "CAPILLARY GC/MS-COMPUTER IDENTIFICATION OF PESTICIDE METABOLITES AND CONFIRMATION OF PESTICIDE RESIDUES" @default.
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- W1903441 doi "https://doi.org/10.1016/b978-0-08-029225-0.50015-1" @default.
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