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- W1919514281 abstract "The azido-tetrazolo tautomerizations of 3,6-diazido-1,2,4,5-tetrazine (DIAT) in different solvents were investigated with HPLC and 13C NMR spectroscopy. 6-Amino-tetrazolo[1,5-b]-1,2,4,5-tetrazine (ATTZ) was irreversibly formed as the final product by azido-cyclization following N2 elimination from one of the azido substituents at room temperature in DMSO. The structure of ATTZ was characterized by X-ray crystallography; differential scanning calorimetry (DSC), mass spectrometry, as well as IR and 1H NMR and 13C NMR spectroscopy. The crystal density was found to be 1.272 g cm−3. DSC result suggested that ATTZ with the melting point of 84 °C strongly decomposes with explosion at 198 °C, which can be regarded as a primary explosive." @default.
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- W1919514281 date "2015-09-04" @default.
- W1919514281 modified "2023-09-24" @default.
- W1919514281 title "Study on the Azido-Tetrazolo Tautomerizations of 3,6-Bis(azido)-1,2,4,5-tetrazine" @default.
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- W1919514281 doi "https://doi.org/10.1002/prep.201500127" @default.
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