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- W1925690923 abstract "We describe a liquid-chromatographic procedure for amoxapine and 8-hydroxyamoxapine, its active metabolite, in serum. We used a mu-Bondapak C18 reversed-phase column and a mobile phase of acetonitrile/water (74/26 by vol) plus 26 microL of n-butylamine per liter. The compounds were measured at 254 nm, with 8-methoxyloxapine as internal standard. Necessary pre-analysis purification consisted of adsorbing the drug from serum onto extraction columns, eluting with 1-butanol/hexane (1/5 by vol), re-extracting into aqueous acid, and from that re-extracting again into the elution-solvent mixture. We prefer this procedure for monitoring both therapeutic and toxic concentrations of amoxapine, because parent drug and metabolite are measured separately." @default.
- W1925690923 created "2016-06-24" @default.
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- W1925690923 date "1982-10-01" @default.
- W1925690923 modified "2023-09-23" @default.
- W1925690923 title "Liquid-chromatographic determination of amoxapine and 8-hydroxyamoxapine in human serum." @default.
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