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- W192810261 abstract "This chapter describes the fabrication and preliminary tests of a pre-concentrator implemented in silicon using reactive ion etching, SF 6 based, to define the channel microstructure and anodic bonding between silicon and glass to seal up the micro-channels. The proposed innovation is the direct coupling of this pre-concentrator with a glass capillary that will perform the electrophoresis analysis. The immobilization of N-2-aminoethyl-3-aminopropylsilane and pre-concentration of copper (II) was verified by means of potentiometric stripping essays, performed with potential and deposition time of 0 V and 120 s, respectively. Pre-concentration of metallic ions aims at environmental applications. The implemented preconcentrator has a pattern, which is similar to that firstly proposed by Regnier and collaborators for electrochromatography applications. The chapter presents the design and implementation of a preconcentrator fabricated on a silicon substrate using silicon micro-channels defined with RIE and sealed with anodic bonding. The fluid injection is achieved by capillarity effects and the surface of the micro-channels is easily modified with defined ligand." @default.
- W192810261 created "2016-06-24" @default.
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- W192810261 date "2003-01-01" @default.
- W192810261 modified "2023-09-26" @default.
- W192810261 title "Silicon microstructure for preconcentration of metallic ions" @default.
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- W192810261 doi "https://doi.org/10.1016/b978-008044046-0.50410-3" @default.
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