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- W1930377013 abstract "A temperature‐controlling device for in‐tube solid‐phase microextraction was developed based on thermoelectric cooling and heating. This device can control the temperature of the capillary column from 0 to 100°C by applying a voltage to a Peltier cooler or stainless steel tube. The extraction temperatures for angiotensin I, propranolol, and ranitidine were optimized. In all cases, setting the temperature to 10°C for extraction achieved the best extraction efficiency. Desorption showed minimum peak broadening at 70°C, contributing to better chromatographic performance. Propranolol was selected as a model compound to compare the performance of temperature‐controlled in‐tube solid‐phase microextraction at optimized conditions. Calibration curves exhibited good linearity ( R 2 > 0.999) over the studied range, and the limit of detection and limit of quantification were about three times lower than those obtained at standard conditions (30°C extraction and desorption)." @default.
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- W1930377013 date "2014-05-15" @default.
- W1930377013 modified "2023-10-06" @default.
- W1930377013 title "Thermoelectric-based temperature-controlling system for in-tube solid-phase microextraction" @default.
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- W1930377013 doi "https://doi.org/10.1002/jssc.201400041" @default.
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