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• W1937248845 abstract "A rapid and straightforward screening protocol of chiral stationary phases (CSPs) in HPLC and SFC resulted in three different methods fit-for-purpose, i.e. analysis and scale-up to semi-preparative enantioselective chromatography. The efficient use of these three methods allowed expedited preparation of an important drug discovery target, (R/S)-1, a potent new sigma 1 (σ1) receptor agonist. The approach taken resulted in significant savings of both time and labor for the isolation of enantiomers compared to the development of a stereo-selective synthesis. The enantiomers of 1 have been isolated allowing studies of their chirooptical properties and an in-deep comparative examination of the pharmacological profile for the individual enantiomers." @default.
• W1937248845 created "2016-06-24" @default.
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• W1937248845 date "2016-01-01" @default.
• W1937248845 modified "2023-09-24" @default.
• W1937248845 title "“Fit-for-purpose” development of analytical and (semi)preparative enantioselective high performance liquid and supercritical fluid chromatography for the access to a novel σ 1 receptor agonist" @default.
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• W1937248845 doi "https://doi.org/10.1016/j.jpba.2015.10.047" @default.
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