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- W1937325393 abstract "A three-step radiosynthesis is described which allows for the first time the preparation of l- and d-3-[18F]fluoro-α-methyltyrosine starting from [18F]fluoride. Corresponding 3-fluoro-4-formyl-benzylated Schöllkopf derivatives were 18F-fluorinated as precursors by isotopic exchange, followed by Baeyer–Villiger oxidation and subsequent hydrolysis of protecting groups in acidic medium. The three-step, two-pot radiosynthesis provided each enantiomer of 3-[18F]fluoro-α-methyltyrosine with an overall radiochemical yield of 32 ± 8% and an enantiomeric excess ≥95% within 140 min in carrier-added form with a molar activity of 20 GBq/mmol." @default.
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- W1937325393 date "2015-10-01" @default.
- W1937325393 modified "2023-09-26" @default.
- W1937325393 title "Stereoselective radiosynthesis of l- and d-3-[18F]fluoro-α-methyltyrosine" @default.
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- W1937325393 doi "https://doi.org/10.1016/j.jfluchem.2015.07.015" @default.
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