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- W1937384303 abstract "Abstract Isopropenyl methyl ketone was polymerized with γ‐ray radiation and with phenylmagnesium iodide in toluene. The polymers obtained with phenylmagnesium iodide as catalyst were separated into methyl ethyl ketone‐soluble and ‐insoluble parts. The soluble parts were amorphoas, while the insoluble parts were crystalline. Treatment of the polymers by heat, alkali and chlorinated solvents induced aldol condensation. It was confirmed by infrared and ultraviolet spectrometry that the crystalline polymer underwent aldol condensation between adjacent units more easily than the amorphous polymer at temperatures lower than 180°C, forming monocyclic structures predominantly, whereas the amorphous polymer resisted in the earlier stage of heating but was more rapidly degraded between 180‐260°C than the crystalline polymer. The length of the conjugated double bond sequences produced in the amorphous polymer showed random distribution." @default.
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- W1937384303 date "1967-12-22" @default.
- W1937384303 modified "2023-10-17" @default.
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- W1937384303 doi "https://doi.org/10.1002/macp.1967.021100119" @default.
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