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- W1948947988 abstract "The X-ray structures of the compounds were solved by direct methods from diffractometer data. 4d: 2-thia-3,3-dimethyl-4R-(t-butyloxycarbonylmethylene)carboxylate-5,7-diaza-6-oxo-8R-phenylacetamido-bicyclo-1R-[3,3,0]octane, C22H29N3O6S, monoclinic, space group P21; cell dimensions: a=13.625(6), b=8.344(3), c=10.656(3)Å, β=95.18(3)°; V=1206.4(8)Å3, Dx=1.28 gcm−3 for Z=2. 1646 measured and 1098 observed reflections. Final R=0.067. 5d: 2-thia-3,3-dimethyl-4R-(t-butyloxycarbonylmethylene)carboxylate-5,7-diaza-6-oxo-7-benzoyl-8R-phenylacetamido-bicyclo-1R-[3,3,0]octane, C29H33N3O7S. H2O, monoclinic, space group P21; cell dimensions: a=11.074(4), b=6.255(1), c=21.801(6)Å, β=92.49(3)°; V=1508.5(8)Å3; Dx=1.29 gcm−3 for Z=2.2257 measured and 1836 observed reflections. Final R: 0.071. Small but significant changes of bond lengths in the diaza pentagonal cycle are probably due to the benzoyl substituent." @default.
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- W1948947988 date "2010-09-01" @default.
- W1948947988 modified "2023-09-27" @default.
- W1948947988 title "X-ray Diffraction Analysis of New ring-Enlargement Derivatives of Penicillin G: 2-thia-3,3-Dimethyl-4R-(t-Butyloxycarbonylmethylene) Carboxylate-5,7-Diaza-6-Oxo-8r-Phenylacetamido-Bicyclo-1r-[3,3,0]Octane and 2-Thia-3,3-Dimethyl-4R-(t-Butyloxycarbonylmeth" @default.
- W1948947988 cites W2048964024 @default.
- W1948947988 doi "https://doi.org/10.1002/bscb.19860950403" @default.
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