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- W196277535 abstract "X-ray fluorescence was applied to the determination of Pb/sup 2+/, Bi/ sup 3+/, Hg/sup 2+/, and Sr separated by paper electrophoresis with the soivent system using buffered 2,2'diaminodiethyl ether N,N'-tetraacetic acid as previousiy described by Wenger, et al. (Mikrochim. Acta, 184(1962)). The method is useful for estimating small amounts of these metal ions; with amounts between 10 and 100 mu g the accuracy is plus or minus 10%. This method has advantages over the colorimetric method, which requires specially treated paper. Electrophoretic separation of Pb and Bi is best carried out in pH 2.05 buffer for 30 min at 20 v/cm potential gradient. Under these conditions Pb migrates to the cathode and Bi toward the anode. The cations are detected on the paper with H/ sub 2/S. Pb and Sr ions are optimally separated with pH 5.03 buffer, and Sr is detected with rhodizonic acid. (H.H.D.)" @default.
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- W196277535 date "1962-05-01" @default.
- W196277535 modified "2023-09-27" @default.
- W196277535 title "X-RAY FLUORESCENCE AS AN AUXILIARY METHOD TO PAPER ELECTROPHORESIS" @default.
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