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• W1963114210 abstract "The nanoflower lead(II) coordination compound {[Pb(phen)(μ-CH3COO)][PF6]}n (1) (phen = 1,10-phenanthroline) was synthesized by a sonochemical method. The nanostructure was characterized by using scanning electron microscopy (SEM), X-ray powder diffraction, elemental analysis, and thermal analysis. The single-crystal X-ray structure shows that the overall structure of 1 is a 1D coordination polymer. Complex 1 has a bridging acetate pathway. Three halogen bonds observed in the structure and the strong halogen bonding of F–Pb causes chemical activity of the lead electron pair. This is further extended into a 3D supramolecular structure by weak π–π intermolecular interactions. The coordination number of the lead(II) ions is six, resulting in PbN2O4. PbO nanoparticles were obtained by the thermolysis of 1 at 180 °C with oleic acid as a surfactant. The morphology and size of the prepared PbO nanoparticles were further observed using scanning electron (SEM) and transmission electron microscopy (TEM), and were analyzed by X-ray photoelectron spectroscopy (XPS)." @default.
• W1963114210 created "2016-06-24" @default.
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• W1963114210 date "2015-09-03" @default.
• W1963114210 modified "2023-10-01" @default.
• W1963114210 title "Effects of Halogen Bonding in Chemical Activity of Lead(II) Electron Pair: Sonochemical Synthesis, Structural Studies, and Thermal Analysis of Novel Lead(II) Nano Coordination Polymer" @default.
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• W1963114210 doi "https://doi.org/10.1002/zaac.201500250" @default.
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