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- W1963673034 abstract "Abstract The electrochemical reduction of CH2(Br)CH2COOEt(I) and CH3CH(Br)CH2CH2COOEt(II) in dimethylformamide solutions containing Et4NclO4 as supporting electrolyte was studied by means of polarography, cyclic voltammetry and coulometry at mercury, gold and vitreous carbon electrodes. CH3CH2COOEt(III), CH2=CHCOOEt(IV) and (CH2CH2COOEt)2(V) were obtained from the electroreduction of (I) at an Hg pool, and CH3(CH2)3 COOEt(VI), CH3-CH=CHCH2COOEt(VII) and (CH3−CH−CH2CH2COOEt)2(VIII) were formed from (II) under the same conditions. The percentage ratio among the various products depends on the potential, the proton donor presence and the nature of the ester treated (I or II). The feasibility of the indirect reduction of (I) and (II) by means of anion radicals of aromatic hydrocarbons was studied; evidence for a different behaviour of (I) and (II) was obtained." @default.
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- W1963673034 date "1981-09-01" @default.
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- W1963673034 title "Direct and indirect reduction of ethyl β-bromopropionate and ethyl γ-bromovalerate in DMF solutions" @default.
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- W1963673034 doi "https://doi.org/10.1016/s0022-0728(81)80427-5" @default.
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