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• W1963884906 endingPage "2285" @default.
• W1963884906 startingPage "2282" @default.
• W1963884906 abstract "Chemoselective catalytic oxidation from 1,2-diols to α-hydroxy acids in a cat. TEMPO/cat. NaOCl/NaClO2 system has been achieved. The use of a two-phase condition consisting of hydrophobic toluene and water suppresses the concomitant oxidative cleavage. A study of the mechanism suggests that the observed selectivity is derived from the precise solubility control of diols and hydroxy acids as well as the active species of TEMPO. Although the oxoammonium species TEMPO+Cl– is hydrophilic, the active species dissolves into the organic layer by the formation of the charge-transfer (CT) complex TEMPO–ClO2 under the reaction conditions." @default.
• W1963884906 created "2016-06-24" @default.
• W1963884906 creator A5036487279 @default.
• W1963884906 creator A5048247150 @default.
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• W1963884906 date "2015-04-17" @default.
• W1963884906 modified "2023-10-03" @default.
• W1963884906 title "Chemoselective Catalytic Oxidation of 1,2-Diols to α-Hydroxy Acids Controlled by TEMPO–ClO₂ Charge-Transfer Complex" @default.
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• W1963884906 doi "https://doi.org/10.1021/acs.orglett.5b01003" @default.
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