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- W1963913370 abstract "Abstract Reaction of [η 5 : η 5 -C 10 H 8 ][CpZrX 2 ] 2 (X = halide) with (η 3 -C 3 H 5 )MgCl in THF at room temperature allowed the isolation and characterization of anti -[η 5 : η 5 -C 10 H 8 ][CpZr(η 1 -CH 2 CHCH 2 (η 3 -CH 2 CHCH 2 )] 2 ( 4b ) in good yield and crystalline form. Crystal data for 4b are as follows: monoclinic, P 2 1 / c , a = 7.990(1), b = 18.522(3), c = 18.272(1) A, β = 93.76(1)°, V = 2698.2(6) A 3 , Z = 4; least-squares refinement of 268 parameters and 2417 out of 3504 reflections converged to R = 0.056 and R w = 0.070. NMR features suggest that occurrence in solution of rapid intramolecular rearrangements between two possible conformations of the allyl groups observed in the solid state structure." @default.
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- W1963913370 date "1991-10-01" @default.
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- W1963913370 title "A binuclear zirconium fulvalene tetraallyl complex. The preparation and the molecular structure of [η5 : η5-C10H8][CpZr(η1-CH2CHCH2)(η3-CH2CHCH2)]2" @default.
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- W1963913370 doi "https://doi.org/10.1016/0022-328x(91)86365-w" @default.
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