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• W1963941128 abstract "Abstract The newly prepared complexes with stoichiometries [Fe(oda)(phen)Cl] (1), [Fe(oda)(4-picNO)(H2O)Cl)] (2) and [Fe2(oda)2(H2O)2Cl2] (3) [H2oda = oxydiacetic acid, phen = 1,10′-phenantroline and 4-picNO = 4-picoline-N-oxide] were synthesized under varying experimental conditions. The complexes were characterized by spectral (IR, FAB-MS and Mossbauer), electrochemical and thermal studies. 57Fe-Mossbauer spectral data for complexes exhibit a quadrupole splitting confirming the presence of iron nuclei in asymmetric environment. The relevant parameters like isomer shift (δ), quadruple splitting (ΔEQ), line widths and peak height ratio (HWh/HWl) are consistent with high spin state of Fe(III) centre with the presence of Kramer’s double degeneracy in distorted octahedral environment. The electrochemical studies indicate existence of quasi-reversible redox couples (FeII/III) in solution." @default.
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• W1963941128 date "2014-04-01" @default.
• W1963941128 modified "2023-09-25" @default.
• W1963941128 title "Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand: 57Fe-Mössbauer and cyclic voltammetric studies" @default.
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• W1963941128 doi "https://doi.org/10.1016/j.molstruc.2014.01.072" @default.
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