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- W1963990475 abstract "The theoretical and practical principles of direct spontaneous voltammetry and spontaneous voltammetric titrations were discussed and the direct determinations of Hg(II), Ag(I), cyanide ion and EDTA were investigated. The spontaneous titrations investigated were: (i) direct complexation, such as the titrations involving Hg(II)-EDTA system ; (ii) indirect complexation, such as the titration of Ag(I) with EDTA; (iii) oxidation-reduction, such as the titration of ferrous ion with permanganate, and (iv) precipitation, such as the titration of cyanide ion with Ag(I). The mechanism, of electrode reactions at the D.M.E. in the titration of Ag(I) with EDTA was explained. In this instance, the end-point of the titration, obtained by the intersection of the titration curve with the zero current, does not correspond to the stoichiometric end-point but to the ratio of the diffusion current constants of the species involved. This is true for all cases where the reaction between the active constituents occurs at the electrode surface. A stoichiometric end-point is obtained only when the active constituents react in the bulk of the solution." @default.
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- W1963990475 date "1966-04-01" @default.
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- W1963990475 title "Spontaneous voltammetry and voltammetric titrations" @default.
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- W1963990475 doi "https://doi.org/10.1016/0022-0728(66)80091-8" @default.
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