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- W1964426102 abstract "A clinically useful method is described for the quantitative analysis of platinum species derived from cis-dichlorodiammineplatinum(II) in urine. The drug and its biodegradation products are derivatized directly in urine by reaction with sodium diethyldithiocarbamate (DDTC) to form a common product, a 2:1 DDTC-platinum adduct. This complex is stable and can be quantitatively extracted into 0.1 volumes of chloroform. An aliquot of the chloroform layer is then subjected to high-performance liquid chromatography on a μBondapak CN column and the eluent monitored spectrophotometrically at 254 nm. At this wavelength the DDTC-platinum adduct has a molar absorptivity of 43,000, and platinum levels of 25 ng/ml of urine can be detected with a precision of ± 2.5% and an accuracy of ±4%." @default.
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- W1964426102 date "1979-05-01" @default.
- W1964426102 modified "2023-10-16" @default.
- W1964426102 title "Urine analysis of platinum species derived from cis-dichlorodiammineplatinum(II) by high-performance liquid chromatography following derivatization with sodium diethyldithiocarbamate" @default.
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- W1964426102 doi "https://doi.org/10.1016/s0021-9673(00)92301-x" @default.
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