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- W1964579459 abstract "A new convenient route for the synthesis of poly(ɛ-caprolactone) (PCL) with α,ω-telechelic diols' end-groups is presented. Synthesis of α,ω-telechelic PCL diols (HOPCLOH) was achieved by ring-opening polymerization (ROP) of ɛ-caprolactone (CL) catalyzed with ammonium decamolybdate (NH4)8[Mo10O34] and using diethylene glycol (DEG) as initiator. Obtained HOPCLOH was characterized by 1H and 13C NMR, FT-IR, GPC and MALDI-TOF. Comparative studies demonstrate that ammonium decamolybdate (NH4)8[Mo10O34] is better catalyst than Sn-octanoate (SnOct2) toward CL polymerization in presence of DEG, under the conditions tested. A biodegradable poly(ester-urethane-urea) derivative was efficiently prepared from synthesized HOPCLOH. Obtained polymer shows minor differences with respect to the properties recorded for a poly(ester-urethane-urea) obtained from commercial HOPCLOH." @default.
- W1964579459 created "2016-06-24" @default.
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- W1964579459 date "2006-12-01" @default.
- W1964579459 modified "2023-10-17" @default.
- W1964579459 title "A novel route to α,ω-telechelic poly(ɛ-caprolactone) diols, precursors of biodegradable polyurethanes, using catalysis by decamolybdate anion" @default.
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- W1964579459 doi "https://doi.org/10.1016/j.polymer.2006.10.023" @default.
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