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- W1964858941 abstract "Im System Ca—Ni—Si wurden die neuen Verbindungen CaNi2Si und Ca3Ni3Si2 hergestellt und ihre Strukturen röntgenographisch an Einkristallen bestimmt. CaNi2Si kristallisiert in der Raumgruppe P63/mmc (Nr. 194) mit den Gitterparametern a = 400, 38(5) pm, c = 988, 6(2) pm und Z = 2 (R1 = 0, 0307, wR2 = 0, 0553 für alle gemessenen symmetrieunabhängigen Reflexe) als Besetzungsvariante des ReB3-Typs. Für Ca3Ni3Si2 wurde eine orthorhombische Zelle mit der Raumgruppe Pnma (Nr. 62), Z = 4 und den Gitterparametern a = 926, 59(5) pm, b = 396, 69(2) pm, c = 1814, 1(2) pm gefunden (R1 = 0, 0435, wR2 = 0, 0605 für alle gemessenen symmetrieunabhängigen Reflexe). Ni und Si bilden gefaltete zweidimensional unendliche Schichten, die durch die Ca-Atome separiert werden. New Compounds in the System Ca/Ni/Si The new compounds CaNi2Si and Ca3Ni3Si2 were synthesized in the Ca—Ni—Si-system and their structures determined by single crystal X-ray diffraction. CaNi2Si crystallizes in the space group P63/mmc (no. 194) with the lattice parameters a = 400.38(5) pm, c = 988.6(2) pm and Z = 2 (R1 = 0.0307, wR2 = 0.0553 for all symmetry-independent reflections) in a site occupancy variant of the ReB3 type. The unit cell of Ca3Ni3Si2 was found to be orthorhombic with a = 926.59(5) pm, b = 396.69(2) pm and c = 1814.1(2) pm (Pnma, no. 62, Z = 4, R1 = 0.0435, wR2 = 0.0605 for all symmetry-independent reflections). The nickel and silicon atoms build puckered two dimensional layers which are separated by the calcium atoms." @default.
- W1964858941 created "2016-06-24" @default.
- W1964858941 creator A5031472552 @default.
- W1964858941 date "2002-09-01" @default.
- W1964858941 modified "2023-09-24" @default.
- W1964858941 title "Neue Verbindungen im System Ca/Ni/Si" @default.
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