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• W1964995497 abstract "Die Alkalimetalladdukte aromatischer Kohlenwasserstoffe 4 (z. B. Naphthalin, Phenanthren oder Anthracen) eignen sich zur Herstellung der anionischen Metallcarbonyl-Komplexe 2 aus den zwei-kernigen Komplexen 1. So ist in präparativem Maßstab auch Natrium-carbonylcyclopentadienyl-niccolat (2e) zu erhalten, mit dem neue Derivate des Carbonylcyclopentadienylnickels (z. B. das Triphenylzinn-Derivat 9a sowie die Acylkomplexe 9b — d) zugänglich werden. Für leichter reduzierbare Komplexe sind Benzophenon-lithium (4d-Li) oder das Dilithium-Addukt 6 des Benzophenons verwendbar, die sich besonders zur Reduktion von Pentacarbonyleisen (5) zum Tetracar-bonylferrat (7) eignen. Preparation of Anionic Transition Metal Complexes by Alkali Metal Adducts of Aromatic Hydrocarbons The alkali metal adducts of aromatic hydrocarbons 4 (such as naphthalene, phenanthrene or anthracene) are reagents for reducing dinuclear complexes 1 to anionic metalcarbonyl complexes 2. By this method sodium carbonylcyclopentadienylniccolate (2e) can also be obtained on a preparative scale, thus providing an entry to new derivatives of carbonylcyclopentadienyl-nickel (such as the triphenyltin derivative 9a, and acyl complexes 9b—d). For more easily reducible complexes, benzophenone-lithium (4d-Li) or the dilithium adduct 6 of benzophenone can be used, which are especially suited for the reduction of pentacarbonyliron (5) to tetracarbonylferrate (7)." @default.
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• W1964995497 date "1980-02-29" @default.
• W1964995497 modified "2023-10-09" @default.
• W1964995497 title "Herstellung anionischer übergangsmetall-Komplexe" @default.
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• W1964995497 doi "https://doi.org/10.1002/jlac.198019800208" @default.
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