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- W1965027720 abstract "Abstract Reaction of [Ru 3 (CO) 12 with (CF 3 ) 2 PP(CF 3 ) 2 in p -xylene at 140°C yielded the compounds [Ru 4 (CO) 13 {μ-P(CF 3 ) 2 } 2 ] ( 1 ), [Ru 4 (CO) 14 {μ-P(CF 3 ) 2 } 2 ] ( 2 ) and [Ru 4 (CO) 11 {μ-P(CF 3 ) 2 } 4 ] ( 3 ). Reaction with [(μ-H) 4 Ru 4 (CO) 12 ] under similar conditions yielded [(μ-H) 3 Ru 4 (CO) 12 {μ-P(CF 3 ) 2 }] ( 4 ). All four compounds have been characterised by X-ray crystallography. The fluxional behaviour of the hydrides in 4 has also been studied by variable-temperature NMR spectroscopy. Compounds 1, 2 and 4 were also obtained from the reactions of Ru 3 (CO) 12 with (CF 3 ) 2 PH in dichloromethane at 80°C." @default.
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- W1965027720 date "1996-03-01" @default.
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- W1965027720 title "Reactions of tetrakis(trifluoromethyl) diphosphine and bis(trifluoromethyl) phosphine with ruthenium carbonyl clusters; X-ray structure of tetraruthenium carbonyl cluster derivatives" @default.
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- W1965027720 doi "https://doi.org/10.1016/0022-328x(95)05886-t" @default.
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