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• W1965156944 endingPage "2813" @default.
• W1965156944 startingPage "2807" @default.
• W1965156944 abstract "A variety of solid-state NMR techniques were applied in order to assign resonances in the 29Si and 23Na NMR spectra of a new crystalline silicate to crystallographically distinct silicon and sodium sites, respectively. Mu-11 is a zeolite-like material with a 1D channel system occupied by water and sodium cations whose framework contains both bridging and non-bridging oxygens. The observed 29Si isotropic chemical shifts did not allow a direct assignment. A preliminary assignment based on the electronegativities calculated for the four ligands around each silicon was supported by correlations between the extent of the distortion from an ideal tetrahedron and the measured chemical shift anisotropy for the different Si sites. 1H–29Si cross polarization experiments confirmed the assignments. The two crystallographically different sodium atoms were resolved by 23Na 3Q-MAS NMR, and an assignment for these two sites is proposed." @default.
• W1965156944 created "2016-06-24" @default.
• W1965156944 creator A5004278388 @default.
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• W1965156944 date "2000-01-01" @default.
• W1965156944 modified "2023-10-17" @default.
• W1965156944 title "Structural characterization of the new porous sodium silicate Mu-11 by 29Si and 23Na solid-state NMR" @default.
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• W1965156944 doi "https://doi.org/10.1039/b002194f" @default.
• W1965156944 hasPublicationYear "2000" @default.
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