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- W1965161838 abstract "Abstract The copper(II), nickel(II), palladium(II) and oxovanadium(IV) chelates of N,N′-ethylenebis (1,1,1-trifluoro-6-methyl-2- oxoheptan-4-imine) (H2TFIVA2en) and N,N′-1,2-propylenebis(1,1,1-trifluoro-6-methyl-2-oxoheptan-4-imine) (H2TFIVA 2pn) were eluted from gas chromatographic columns, but their copper and nickel chelates could not be resolved. The detection limits were found to be 4–40 ng for each metal chelate. The copper, nickel, palladium and oxovanadium chelates were separated on reserved-phase HPLC columns, Nova Pak C18 (150 × 3.9 mm) and Microsorb C18, (150 × 4.6 mm). Elution was obtained with a binary mixture of methanol-water or a ternary mixture of methanol-acetonitrile-water. Detection was achieved using a UV detector. Linear calibrations were obtained over the range 10–1200 ng and detection limits were 0.4–4.0 ng for the metal chelates." @default.
- W1965161838 created "2016-06-24" @default.
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- W1965161838 date "1993-06-01" @default.
- W1965161838 modified "2023-09-24" @default.
- W1965161838 title "Gas and liquid chromatographic studies of copper(II), nickel(II), palladium(II) and oxovanadium(IV) chelates of some fluorinated ketoamine Schiff bases" @default.
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- W1965161838 doi "https://doi.org/10.1016/0021-9673(93)80279-h" @default.
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