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- W1965632113 abstract "The monomeric homoleptic Pt(0) complex [Pt(GaCp*)4] (1) has been synthesized by reaction of [Pt(COD)2] with GaCp* in hexane. The monomeric homoleptic Pd(0) complexes [Pd(GaCp*)4] (2) and [Pd{InC(SiMe3)3}4] (3) are accessible by reaction of [Pd(tmeda)(CH3)2] with GaCp* and [InC(SiMe3)3], respectively. These reactions were shown to proceed via methyl group transfer from palladium to indium or gallium, respectively. Complexes 1 and 2 can be used as building blocks for the synthesis of dinuclear cluster compounds. Thus, reaction of [Pt(COD)2] with 1 or 2 and subsequent addition of GaCp* yields [Pt2(GaCp*)2(μ2-GaCp*)3] (4a) and [PtPd(GaCp*)(μ2-GaCp*)3] (5a). Intermediates of this dimerization reactions, i.e., [Pt2(GaCp*)(μ2-GaCp*)3(η2-COD)] (4b) and [PtPd(GaCp*)(μ2-GaCp*)3(η2-COD)] (5b), were isolated and characterized by means of variable-temperature NMR spectroscopy." @default.
- W1965632113 created "2016-06-24" @default.
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- W1965632113 date "2003-05-21" @default.
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- W1965632113 title "[M(GaCp*)<sub>4</sub>] (M = Pd, Pt) as Building Blocks for Dimeric Homoleptic Cluster Compounds of the Type [MPt(GaCp*)<sub>5</sub>]" @default.
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- W1965632113 doi "https://doi.org/10.1021/om021003i" @default.
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