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- W1965944650 abstract "Monovanadium derivatives of 12-molybdosulfate(VI) and 18-molybdodisulfate(VI), [S(VMo11)O40]3− and [S2(VMo17)O62]5−, have been prepared as tetrabutylammonium (n-Bu4N+) salts from a Mo(VI)–V(V)–H2SO4–CH3CN system. Both mixed molybdosulfate(VI) comlexes were characterized by their IR and UV spectra and their voltammetric behaviors. These mixed complexes are stable in nonaqueous solutions. In a 90% (v/v) CH3CN–0.1 M (M = mol dm−3) HClO4 system, the [S(VMo11)O40]3− anion transforms spontaneously into 12-molybdovanadate(V), whereas the [S2(VMo17)O62]5− anion is stable. In a 90% (v/v) CH3CN–0.5 M HClO4 system, on the other hand, both mixed complexes change into 18-molybdodisulfate(VI), [S2Mo18O62]4−." @default.
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- W1965944650 date "1992-03-01" @default.
- W1965944650 modified "2023-09-27" @default.
- W1965944650 title "Synthesis and Characterization of Vanadium-Substituted Heteropoly Molybdosulfate(VI) Complexes" @default.
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- W1965944650 doi "https://doi.org/10.1246/bcsj.65.799" @default.
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