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- W1966129196 abstract "Abstract The phase diagrams in the PbO–Nb 2 O 5 system and the PbO–Ta 2 O 5 system depict pyrochlore structure at certain molar ratios. Compositions Pb 2 Nb 1.51 Pb 0.49 O 6.30 (1), Pb 2 Ta 1.4 Pb 0.6 O 6.21 (2), and Pb 2 Ta 1.25 Pb 0.75 O 6.57 (3) belonging to this family, are refined in the cubic space group Fd 3 m ( Z =8; lattice parameter a =10.762(1), 10.744(1), 10.757(5) A, respectively) using the Rietveld refinement approach. The analyses suggest that the B-site is partially occupied by Pb leading to the general formula Pb 2 ( M 2− y Pb y )O 7− δ (0.0 y M =Nb or Ta). There is an overall broadening observed in the X-ray peak widths in 1, 2, and 3 compared to the Pb-deficient parent phases. It is observed that the X-ray peak widths of 2 is broad, while 3 displays narrow peak widths. It is found via strain analysis that the line broadening observed correlates with the strain in the lattice." @default.
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- W1966129196 date "2001-01-01" @default.
- W1966129196 modified "2023-09-27" @default.
- W1966129196 title "X-ray Structure Refinements and Strain Analysis of Substituted Cubic Lead Pyrochlores Pb2(M2−yPby)O7−δ(0.0<y<0.8; M=Nb or Ta)" @default.
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- W1966129196 doi "https://doi.org/10.1006/jssc.2000.8983" @default.
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