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• W1966247825 endingPage "1012" @default.
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• W1966247825 abstract "The synthesis and preliminary solution phase ion binding properties of the N-tosylpyrrolidine calix[4]pyrrole 2 are reported. This β-octaalkyl-substituted calix[4]pyrrole, the first to be prepared via a direct condensation reaction, was obtained by reacting the 3,4-alkyl-functionalized pyrrole 8 with acetone in the presence of an acid catalyst. On the basis of 1H NMR spectroscopic analyses and isothermal titration calorimetry, it was concluded that, compared with the parent, β-unsubstituted calix[4]pyrrole (1), compound 2 possesses significantly enhanced binding ability for halide anions in chloroform. Furthermore, 2 proved capable of solubilizing in chloroform solution the otherwise insoluble salts, CsF and CsCl. These effects are ascribed to the interactions between the four tosyl groups present in 2 and the counter cations of the halide anion salts." @default.
• W1966247825 created "2016-06-24" @default.
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• W1966247825 date "2010-12-09" @default.
• W1966247825 modified "2023-10-17" @default.
• W1966247825 title "<i>N</i>-Tosylpyrrolidine Calix[4]pyrrole: Synthesis and Ion Binding Studies" @default.
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• W1966247825 doi "https://doi.org/10.1021/jo101882r" @default.
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