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- W1966248717 abstract "High temperature H{sub 2}-annealing of Ni-25Cr specimens reduced the average sulfur content in the alloy to less than 0.05 ppmwt, but resulted in a sulfur gradient in the treated samples, where a 10-fold higher concentration exists in the bulk of the sample than in the near-surface region. Cr{sub 2}O{sub 3} scales that developed in the H{sub 2}-annealed samples ere initially more adherent than those formed on the untreated alloy. However, due to the presence of the sulfur gradient, small amounts of sulfur slowly diffused to the scale/alloy interface via alloy grain boundaries. This caused the first-formed chromia scale to detach and buckle above these boundaries, and the scale eventually failed by localized spallation. The growth rate of the chromia scale was not affected by the removal of sulfur, but the formation of Ni-rich nodules through the Cr{sub 2}O{sub 3} layer was eliminated. As sulfur from the bulk diffused towards the scale/alloy interface, Ni-rich nodules also began to develop. The growth of these nodules is believed to be associated with Ni outward diffusion through defects in the first-formed chromia layer. A more defect-free scale seems to have developed by eliminating impurities in the alloy." @default.
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- W1966248717 date "1995-11-01" @default.
- W1966248717 modified "2023-09-27" @default.
- W1966248717 title "Effect of sulfur removal by H2-annealing on the oxidation behavior of a Ni-25Cr alloy" @default.
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- W1966248717 doi "https://doi.org/10.1016/0956-716x(95)00385-9" @default.
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