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• W1966274585 abstract "Treatment of tetrakis(dimethylamido)titanium(IV) and tetrakis(diethylamido)titanium(IV) with two equivalents of 1,3-diphenyltriazene in hexane afforded bis(dimethylamido)bis(1,3-diphenyltriazenido)titanium(IV) (62%) and bis(diethylamido)bis(1,3-diphenyltriazenido)titanium(IV) (68%), respectively, as deep red crystalline solids. Reaction of tetrakis(dimethylamido)titanium(IV) with more than two equivalents of 1,3-diphenyltriazene in refluxing toluene did not lead to substitution of more than two dimethylamido ligands, but only gave extensive decomposition. Treatment of tetrakis(dimethylamido) zirconium(IV) with four equivalents of 1,3-diphenyltriazene in hexane afforded tetrakis(1,3-diphenyltriazenido)-zirconium(IV) (79%) as a deep red crystalline solid. Crystal structures of bis(dimethylamido) tetrakis(1,3-diphenyltriazenido)zirconium(IV) were determined. The titanium complexes exhibit octahedral coordination spheres with cis-dialkylamido ligands, while the zirconium complex is eight-coordinate with η2-1,3-diphenyltriazenido ligands. Solution molecular weight measurements for tetrakis(1,3-diphenyltriazenido)zirconium(IV) indicated a monomeric structure in benzene, consistent with the structural results." @default.
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• W1966274585 date "1997-09-01" @default.
• W1966274585 modified "2023-09-28" @default.
• W1966274585 title "Synthesis and characterization of titanium and zirconium complexes bearing diphenyltriazenido ligands" @default.
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• W1966274585 doi "https://doi.org/10.1016/s0277-5387(97)00189-7" @default.
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