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• W1966393425 abstract "The variations in the capacitance of Ti/SnO2–Sb–Mn/β-PbO2 electrodes prepared using sol–gel and electrodeposition techniques with various calcination temperatures and molar ratios of tin and manganese are discussed in this work. The microscale morphology and physical composition of the fabricated electrodes were characterized by scanning electron microscopy and X-ray diffraction. Cyclic voltammetry and galvanostatic charge–discharge tests were also performed to evaluate the electrochemical performance. The experimental data showed that the capacitance of prepared Ti/SnO2–Sb–Mn/β-PbO2 electrodes was inversely related to the calcination temperature and the molar ratio of tin and manganese in the molding process of the transition layer. The optimal sintering temperature and Sn/Mn molar ratio were 550 °C and 4:1, respectively, while the specific capacitance was 36.35 mF cm−2 at a charge–discharge current density of 1.0 mA cm−2 in a phenolic electrolyte. In addition, the mechanism for improving the capacitance during phenol electro-oxidation in the presence of Mn was investigated by comparing the electrochemical impedance spectra of the Ti/SnO2–Sb–Mn/β-PbO2 electrode with those of the Ti/SnO2–Sb/β-PbO2 electrode. A larger electrolyte resistance, accompanied by a smaller charge-transfer resistance, was obtained for the electrode with Mn doping, which could be ascribed to the decrease in electrical conductivity and increase in electron-capture capacity of MnOx." @default.
• W1966393425 created "2016-06-24" @default.
• W1966393425 creator A5023297657 @default.
• W1966393425 creator A5031498126 @default.
• W1966393425 creator A5067279934 @default.
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• W1966393425 date "2015-06-01" @default.
• W1966393425 modified "2023-10-09" @default.
• W1966393425 title "Effect of calcination temperature and molar ratio of tin and manganese on capacitance of Ti/SnO2–Sb–Mn/β-PbO2 electrode during phenol electro-oxidation" @default.
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• W1966393425 doi "https://doi.org/10.1016/j.jelechem.2015.02.029" @default.
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