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• W1966600247 abstract "The clathrate-I phase Cs8–xGe44+y□2–y (space group Pmn) was prepared by high-pressure high-temperature reactions of Cs4Ge4 and α-Ge. Different reaction conditions were found to have a strong influence on the lattice parameter of the clathrate-I phase ranging from 10.8070(2) Å to 10.8493(3) Å. A single crystal with composition Cs8Ge44.40(2)□1.60(2) was obtained from a sample with a = 10.8238(2) Å (niobium ampoule, p = 3.4 GPa, Tmax = 1400 °C). Structure analysis based on X-ray single crystal data shows unambiguously an excess of germanium atoms with respect to the electron balanced composition Cs8Ge44□2 on basis of the Zintl concept." @default.
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• W1966600247 date "2011-07-20" @default.
• W1966600247 modified "2023-09-24" @default.
• W1966600247 title "Preparation and Crystal Structure of the Clathrate-I Cs8-xGe44+y□2-y" @default.
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• W1966600247 doi "https://doi.org/10.1002/zaac.201100187" @default.
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