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- W1966608093 abstract "The room-temperature reaction of (PMe3)2Ni(CH2CMe2-o-C6H4) (3) with 3 equiv of p-tolyl azide (TolN3) results in evolution of N2 and clean formation of the N-p-tolylindoline derivative TolNCH2CMe2-o-C6H4 (4a), isolated in 82% yield. The reaction almost certainly proceeds via insertion of an “NTol” fragment from TolN3 into the Ni−C(aryl) bond to give an intermediate azametallacycle [LnNi(NTol-o-C6H4CMe2CH2)] (5), which then undergoes C,N-reductive elimination to afford the indoline 4a." @default.
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- W1966608093 date "1996-06-11" @default.
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- W1966608093 title "Indoline Synthesis via Coupling of Phenethyl Grignard Reagents with Organoazides Mediated by (Alkylphosphine)nickel(II) Complexes" @default.
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- W1966608093 doi "https://doi.org/10.1021/om960286+" @default.
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