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- W1966659046 abstract "Abstract Cinnamonitrile was synthesized via the environmentally benign liquid-phase dehydration of cinnamaldoxime over Al-MCM-41 modified with H 3 PO 4 . FT-IR experiments with pyridine have indicated that these mesostructured aluminosilicates contain both Bronsted and Lewis acid sites. The catalytic properties of their H 3 PO 4 treated derivatives for dehydration of cinnamaldoxime have been evaluated. An aprotic solvent with a higher dielectric constant was preferred for this transformation. The conversion of cinnamaldoxime to cinnamonitrile increased with increasing the H 3 PO 4 content in the catalysts up to a maximum value of 30% and decreasing if H 3 PO 4 content was higher. The influence of other operating parameters was also investigated." @default.
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- W1966659046 date "2009-02-01" @default.
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- W1966659046 title "Efficient dehydration of cinnamaldoxime to cinnamonitrile over H3PO4/Al-MCM-41" @default.
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- W1966659046 doi "https://doi.org/10.1016/j.catcom.2008.11.036" @default.
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