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• W1966676207 abstract "The manuscript describes a straightforward synthetic route toward a new family of chiral nonracemic dibenzobarrelene-based pincer ligands. The target molecules have been synthesized via lithiation of the racemic 1-bromo-8-diphenylphosphinotriptycene (2) and subsequent quenching with diastereomerically pure (1R,2S,5R)-(–)-menthyl (S)-p-toluenesulfinate. The resulting mixture of diastereomers was resolved using conventional column chromatography. Hydrogenation of the diastereomerically pure compounds lead to the formation of enantiopure PCS ligands." @default.
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• W1966676207 date "2014-01-01" @default.
• W1966676207 modified "2023-10-12" @default.
• W1966676207 title "Synthesis of chiral nonracemic PC(sp3)P pincer ligands" @default.
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• W1966676207 doi "https://doi.org/10.1016/j.jorganchem.2013.10.051" @default.
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