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• W1966774237 abstract "A novel methylene insertion product is reported. The new compound {(CO)3Fe(μ-CH2)Te}2 has been isolated from the reaction of the mixed-chalcogenide compound Fe2(CO)6(μ-STe) with diazomethane. It has been characterized by IR, 1H, 13C and 125Te NMR spectroscopy. Its structure has been determined by single-crystal X-ray diffraction methods: monoclinic; space group, P21/c; a = 6.743(2), b = 10.996(2), c = 18.007(2) Å, β = 96.60(2)°; V = 1326.3(2) Å3; Z = 4; F(000) = 1024; Mo Kα radiation (graphite monochromated); μ = 6.53 mm−1; T = 293 K; Dc = 2.86 g cm−3; R = 0.065 (Rw = 0.064)." @default.
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• W1966774237 date "1995-05-01" @default.
• W1966774237 modified "2023-10-11" @default.
• W1966774237 title "Insertion of methylene group into FeTe bond: synthesis and characterization of {(CO)3Fe(μ-CH2)Te}2" @default.
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• W1966774237 doi "https://doi.org/10.1016/0022-328x(94)05353-d" @default.
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