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- W1966810112 abstract "Abstract The syntheses and characterizations of the phenyl and α-naphthyl analogs of 3-aryl-1,3,5,5-tetramethylcyclohex-l-ene and -6-ene are reported. A detailed study of the proton NMR spectra of these compounds was made and it was found that the spectra were sufficient for the conformational analysis of the synthesized compounds. Despite the presence of two sp2 carbons in the cyclohexene ring system, the aromatic moieties remained strictly in an axial or pseudoaxial disposition. This was borne out by the high degree of resolution of small four-bond “W” couplings between methylene protons and by the observation of large high-field shifts of methyl groups across from the aromatic ring substituent. In the case of the α-naphthyl analogs, it was possible to determine the aromatic ring orientation by observing its diamagnetic ring current effects on the nonaromatic protons of the molecules." @default.
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- W1966810112 date "1973-03-01" @default.
- W1966810112 modified "2023-10-07" @default.
- W1966810112 title "NMR studies of structure and conformation in some highly substituted cyclohexenes I. Synthesis and proton NMR studies" @default.
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- W1966810112 doi "https://doi.org/10.1016/0022-2364(73)90182-0" @default.
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