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- W1966854811 abstract "The hydrogenation properties of CaNi3 were investigated at temperatures ranging from 298 to 773 K by differential thermal analysis (DTA). This compound exhibited four exothermic peaks at 373, 498, 543 and 653 K followed by an endothermic peak at 748 K when the compound was heated to 773 K under a hydrogen atmosphere of 3 MPa, and its final products were CaH2 and Ni. However, the formation of a new ternary hydride was observed in the X-ray diffraction (XRD) profiles below the endothermic reaction temperature at which the final products were formed. The Rietveld refinement of the obtained XRD profiles and a volumetric measurement of the hydrogen content based on the Sieverts’ method indicated that this new phase was CaNiH3 with a cubic CsCl type structure for the metal constituents. The experimental data obtained by XRD and DTA were discussed from the viewpoint of the disproportionation of CaNi3 in the hydrogen atmosphere." @default.
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- W1966854811 date "2002-02-01" @default.
- W1966854811 modified "2023-09-25" @default.
- W1966854811 title "Disproportionation of CaNi3 hydride: formation of new hydride, CaNiH3" @default.
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- W1966854811 doi "https://doi.org/10.1016/s0925-8388(01)01739-x" @default.
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