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- W1966968908 abstract "A1. Crystal structure A1. Polymorphism A1. Recrystallization A1. X-ray diffraction B2. Pharmaceuticals abstract The first crystal structure elucidation of pholcodine monohydrate, an important antitussive active pharmaceutical ingredient is reported herein. The studied compound crystallizes in the orthorhombic system in the space group P212121. Each H2O molecule is shared by two pholcodine molecules via three strong hydrogen bonds. The detailed crystallization screening from several different organic solvents afforded single crystals with various quality, all exhibiting prism-to-needlelike micro morphology. The investigation of the obtained single crystals by means of several physico-chemical, solid-state instru- mental techniques (FT-IR, DSC, TG/DTG and XRPD) proved that pholcodine monohydrate exists in a single crystalline modification, identical to the commercial form of the compound." @default.
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- W1966968908 date "2013-07-01" @default.
- W1966968908 modified "2023-09-26" @default.
- W1966968908 title "Pholcodine monohydrate: Crystal structure and polymorphism" @default.
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- W1966968908 doi "https://doi.org/10.1016/j.jcrysgro.2013.04.031" @default.
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