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• W1967047026 abstract "5,5′-bis(1H-tetrazolyl)amine (BTA), a nitrogen rich molecular solid has been investigated under compression at room temperature. Powder x-ray diffraction using synchrotron radiation and micro-Raman spectroscopy were carried out to pressures up to 12.9 GPa. BTA conserves the crystalline structure of its room condition phase up to the highest pressure, i.e., an orthorhombic unit cell (Pbca). A fit of the isothermal compression data to the Birch-Murnaghan equation of state reveals the high compressibility of BTA. An analysis of the volume change with pressure yields a bulk modulus and its derivative similar to that of high-nitrogen content molecular crystals. Upon laser heating to approximately 1100 K, the sample decomposed while pressurized at 2.1 GPa, resulting in a graphitic compound. Finally, numerical simulations demonstrate that the minimum energy conformation is not experimentally observed since a higher energy conformation allows for a more stable dense packing of the BTA molecules." @default.
• W1967047026 created "2016-06-24" @default.
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• W1967047026 date "2014-05-08" @default.
• W1967047026 modified "2023-09-22" @default.
• W1967047026 title "Dense nitrogen-rich energetic materials: A study of 5,5′-bis(1<i>H</i>-tetrazolyl)amine" @default.
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• W1967047026 doi "https://doi.org/10.1063/1.4870830" @default.
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