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- W1967242543 abstract "Abstract Nitrosyl halides NOX (X = Cl, Br) reacted with osmium carbonyl complexes [OsH(CO)CIL 3 ], [Os(CO)Cl 2 L 3 ] and [OsH 2 (CO)L 3 ] (L = PPh 3 , AsPh 3 ) to give osmium nitrosyl complexes [Os(NO)X 3 L 2 ], [Os(NO)CIBr 2 L 2 ] and [Os(NO)C1 2 BrL 2 ] and osmium carbonyl complexes [Os(CO) 2 X 2 L 2 ] (X = Cl, Br; L = PPh 3 , AsPh 3 ). Low valent osmium nitrosyl complexes [Os(NO)X(AsPh 3 ) 3 ] (X = Cl, Br) were prepared by refluxing [Os(NO)X 3 (AsPh 3 ) 2 ] with excess AsPh 3 . Reaction of sulphur with [Os(NO)X 3 (PPh 3 ) 2 ] resulted in the formation of novel thionitro complexes [Os(NSO)X 2 (PPh 3 ) 2 ]. [Os(NO)C1 3 (PPh 3 ) 2 ] reacted with [Na(S 2 CNR 2 ) · x H 2 O] (R = Et. Me) under different reaction conditions to produce the complexes [Os(NO)Cl 2 (S 2 CNR 2 )(PPh 3 )] and [Os(S 2 CNR 2 ) 3 ]. The products have been characterized by elemental analyses, magnetic measurements, IR and electronic spectral studies." @default.
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- W1967242543 date "1988-01-01" @default.
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- W1967242543 title "Synthesis and reactions of osmium nitrosyl complexes" @default.
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