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- W1967252908 abstract "Abstract The template condensation of alkylacetoacetate with diethylenetriamine resulted in the formation of homodinuclear transition metal complexes of a 20-membered macrocyclic ligand. The overall geometry and the mode of bonding have been inferred with IR, 1 H NMR, EPR and electronic spectra studies as well as magnetic and molar conductance data. An octahedral geometry around the metal ion is suggested for [M 2 L 1 X 2 ] and [M 2 L′ 1 X 2 ] where M = iron(II) and cobalt(II), and X = Cl or NO 3 . A distorted square planar and a tetrahedron geometry is proposed for [M 2 L 2 ]X 2 and [M 2 L′ 2 ]X 2 when M = copper(II0 and zinc(II) respectively; X = Cl or NO 3 . The distortion in the copper complexes is confirmed through EPR investigation." @default.
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- W1967252908 date "1994-05-01" @default.
- W1967252908 modified "2023-09-23" @default.
- W1967252908 title "Synthesis and spectral studies of binuclear transition metal complexes of diamidediimine hexaazamacrocycles" @default.
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- W1967252908 doi "https://doi.org/10.1016/s0277-5387(00)81701-5" @default.
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