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• W1967295655 endingPage "4803" @default.
• W1967295655 startingPage "4787" @default.
• W1967295655 abstract "Despite the large number of metal–organic frameworks that have been studied in the context of post-combustion carbon capture, adsorption equilibria of gas mixtures including CO2, N2, and H2O, which are the three biggest components of the flue gas emanating from a coal- or natural gas-fired power plant, have never been reported. Here, we disclose the design and validation of a high-throughput multicomponent adsorption instrument that can measure equilibrium adsorption isotherms for mixtures of gases at conditions that are representative of an actual flue gas from a power plant. This instrument is used to study 15 different metal–organic frameworks, zeolites, mesoporous silicas, and activated carbons representative of the broad range of solid adsorbents that have received attention for CO2 capture. While the multicomponent results presented in this work provide many interesting fundamental insights, only adsorbents functionalized with alkylamines are shown to have any significant CO2 capacity in the presence of N2 and H2O at equilibrium partial pressures similar to those expected in a carbon capture process. Most significantly, the amine-appended metal organic framework mmen-Mg2(dobpdc) (mmen = N,N′-dimethylethylenediamine, dobpdc 4– = 4,4′-dioxido-3,3′-biphenyldicarboxylate) exhibits a record CO2 capacity of 4.2 ± 0.2 mmol/g (16 wt %) at 0.1 bar and 40 °C in the presence of a high partial pressure of H2O." @default.
• W1967295655 created "2016-06-24" @default.
• W1967295655 creator A5005527509 @default.
• W1967295655 creator A5020637044 @default.
• W1967295655 creator A5028537931 @default.
• W1967295655 creator A5041282926 @default.
• W1967295655 creator A5042591801 @default.
• W1967295655 creator A5063456302 @default.
• W1967295655 creator A5064274249 @default.
• W1967295655 creator A5068448504 @default.
• W1967295655 date "2015-04-06" @default.
• W1967295655 modified "2023-10-06" @default.
• W1967295655 title "Application of a High-Throughput Analyzer in Evaluating Solid Adsorbents for Post-Combustion Carbon Capture via Multicomponent Adsorption of CO₂, N₂, and H₂O" @default.
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